B.E. Chem 3rd Year(Sem6)


B.E.III (CH) 6th Semester Teaching
Scheme
Examination Scheme
Theory Exam
Practical/Quiz/Viva/T.W.
University Exam.
TUT
CONT. EVOLUTION TOTAL MARKS
COURSE NAME COURSE NO L Hrs T Hrs P
Hrs
DUR Hrs MKS DUR Hrs MKS
Gen. Chem. Tech.II
601
3
0
2
3
100
2
50
-
-
150
Chem. Engg. Therm-II
602
3
1
0
3
100
-
-
25
-
125
Chem. Reac.Engg.-I
603
3
1
2
3
100
2
50
25
-
175
Chem. SystemModel.
604
3
0
0
3
100
-
-
-
-
-
Instrumentation
605
3
0
2
3
100
2
50
-
-
155
Mass Transfer – II
606
3
0
4
3
100
2
100
-
-
200
TOTAL
18
2
10
---
600
8
250
50
---
900
Total Contact Hours : 026
Total Marks : 900


B.E. Chemical Engineering 6th Semester

Sr.No.
Subject Name
601
Gen. Chem. Tech.-II
602
Chem. Engg. therm-II
603
Chem. Reac.Engg.-I
604
Chem. SystemModel.
605
Instrumentation
606
Mass Transfer – II


General Chemical Technology – II (Semester –VI)

Name
Details

Teaching Scheme :

L=3; P/D=2; TA=0

Examination Scheme

Theory = 3hours; Marks= 100;

Practical / Drawing :

Internal evaluation Marks: 20; External evaluation Marks: 30; Total Marks: 50

1. Petroleum Refining
2. Petrochemical industry.
3. Polymer industry: Manufacture of phenol and urea formaldehyde resins, PVC, Polyethylene, Synthetic rubber etc.
4. Synthetic fiber industry : Nylon polyester, Acrylics, rayons.
5. Fine Chemicals and drugs : Classification of dyes, Azo dyes, Reactive dyes, disperse dyes.
6. Intermediates & Dyes classification of dyes, Azo dyes, Reactive dyes & Disperse dyes.
7. Bio-chemical Engineering Fundamentals, micro-organisms,strains culture etc., kinetics of biochemical reaction, fermentation aeration.
8. Environmental aspects of various industries.

References:

1 R.N. Shreve, J.A. Brink, “ Chemical Process Industries” 4th edition.International Students edition

2 G.F. Austin . “Shreve’s Chemical Process Industries” 5th edition., Mcgraw Hill Publications G.F. Austin . “Shreve’s Chemical Process Industries” 5th edition., Mcgraw Hill Publications.

3 M.Gopala Rao and M. Sitting, “ Dryden’s Outline of Chemical Technology” 2nd edition., East-West publications
4 Bailey & Ollis, ‘Bio-chemical Engineering Fundamentals’, 2nd edition., International Student Edition.
5 Nelson. ‘Petroleum refinery Processes’, McGraw Hill Publication.

Chemical Engg. Thermodynamics –II (Semester –VI)

Name
Details

Teaching Scheme :

L=3; P/D=0; TA=1

Examination Scheme

Theory = 3hours; Marks= 100;

Practical / Drawing :

Tutorial = 25

Thermodynamic properties of fluids:

Partial molar properties, chemical potential, non-ideal solutions, fugacity, fugacity coefficient, for pure component and for mixture of gases. For liquids- Lewis randall rule, Henry’s law, excess property, activity and activity coefficient.

Phase equilibrium:

Phase rule, Duhem theorem, miscible system, immiscible system, partially miscible systems, testing of vapor liquid equilibrium data, Gibbs Duhem equation, Van laar equation, Margules equation, Redlich kister equation, P-x-y , T-x-y and x-y diagrams, Vapour liquid equilibrium of ideal and nonideal solutions, Raoult’s and Henry’s law.

Chemical equilibrium:

criteria, equilibrium conversion(x), constant(k), effect of temperature and pressure on k, evaluation of k, evaluation of equilibrium conversion for gas phase reaction.

Introduction to Statistical thermodynamics:

Stefan Boltzmann, Bose Einstein and Fermi Dirac distributors, corrected Boltzmann statics, partition functions, etc.

References:

1. J.M.Smith and H.C. Vanness, ‘Introduction to Chemical Engg. Thermodynamics’, 3rd and 4th Ed., MGH.

2. Nag P.K “Engineering ”

3. B.F. Dodge, ‘Chemical Engineering Thermodynamics’, MGH.

Chemical Reaction Engineering – I (Semester –VI)

Name
Details

Teaching Scheme :

L=3; P/D=2; TA=1

Examination Scheme

Theory = 3hours; Marks= 100;

Practical / Drawing :

Internal evaluation Marks: 20; External evaluation Marks: 30; Tutorial: 25; Total Marks:75

1. Introduction: Chemical Kinetics, Classification of reactions, variable affecting reaction.
2. Kinetics of homogenous reactions.
3. Instrumentation of Batch Reactor data.
4. Introduction to Reactor Design : Material and energy balances, single ideal reactor, ideal batch reactor.
5. Design of single reaction : Size comparison of single reactors, batch reactor-mixed versus plug flow reactors, first & second order reactions, Gen. Graphical comparison.
6. Multiple reaction system : Plug flow reactors in series and/or parallel, equal sized mixed reactors, recycle factor.
7. Temperature & pressure effects : Single & Multiple reactions.
8. Industrial applications.

References:

1. Octave Levenspiel , 'Chemical Reaction Enfineering' , 2nd ed. , John-Wiley.

2. J.M. Smith, 'Chemical Engg. Kinetics' , McGraw Hill Co.

Chemical System Modelling (Semester –VI)

Name
Details

Teaching Scheme :

L=3; P/D=2; TA=0

Examination Scheme

Theory = 3hours; Marks= 100;

1. Introduction: Physical and mathematical modelling, principle of similarity, definition of independent variables and dependent variables, boundary conditions.
2. Mathematical modelling of Chem. Engg. Systems: single, two and n-stage extraction steady state mass transfer processes, Un steady state formulations of a single stage extraction, steady state heat conduction through hollow cylindrical pipe using various boundary conditions, unsteady process of steam heating of a liquid, heat transfer through extended surface(triangle and rectangular), steady state counter current cooling of a tank, diffusion with chemical reaction in a tubular reactor etc.
3. Lapalace Transforms: Thermometer systems, mixing tanks, fixed bed reactor formulations
4. Partial differential equations and finite differences; a review
5. Numerical methods: a review
6. Treatment of experimental results
7. Optimization

References:

1. V.G.Jenson and G.V. Jeffers, ‘ Mathematical methods in chemical engineering’, Academic press, NY.

2. H.S. Mickley, T.S. Shrewood and C.E. Reed, ‘Applied mathematics in chemical engineering’, TMGH, New Delhi.

Instrumentation (Semester –VI)

Name
Details

Teaching Scheme :

L=3; P/D=0; TA=0

Examination Scheme

Theory = 3hours; Marks= 100;

Practical / Drawing :

Internal evaluation marks :- 20; External evaluation marks - 30; Total Marks - 50

Instrumentation: Measuring Instruments For Temperature, Pressure, Level And Flow.

Micro-Processor Applications:

1. Micro-processor architecture & instruction set for Intel, Zilog and Motorola.
2. Logic structure, combinational logics.
3. Karnaugh Maps, assembly language programming.
4. Timing diagrams, counter & timing delays, stack & subroutines.
5. Interfacing, parallel & seriel, programmable peripheral interface, interrupts, data conversion.
6. Data conversion – ADC & DAC data logging, microcontrollers, program logic controllers, application to process control and drafting.

References:

1. Donald Eckman, ‘ Industrial Instrumentation ‘.

Mass Transfer-II (Semester –VI)

Name
Details

Teaching Scheme :

L=3; P/D=4; TA=0

Examination Scheme

Theory = 3hours; Marks= 100;

Practical / Drawing :

Internal evaluation Marks: - 25; External evaluation Marks - 75; Total Marks - 100

1. Absorption: Equilibrium, material balances for single component transfer, multistage and packed tower operation.
2. Humidification: Vapor gas mixtures, gas liquid contact operations, adiabatic and nonadiabatic operation.
3. Liquid extraction: stage wise, stage type contactor etc.
4. Adsorption and ion exchange: stagewise operation etc.
5. Drying: Batch drying, mechanism, continuous drying.
6. Leaching: Steady state and unsteady state operations.
7. Crystallization: Equilibria, operations, equipments.
8. Introduction to recent separation techniques using mass transfer.

References:

1. R. E. Treybal, Mass transfer operations, 3rd Edition, McGraw Hill Publication

2. McCabe and Smith, Unit operation in chemical engineering, McGraw Hill Publication





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